Download MendeleyHigh Energy Macromolecular Crystallography Enables Data Collection at Room Temperature
Jakoncic, J., Stojanoff, V., Honkimaki, V.To be published.
4B5L
The 1.6 A High Energy Room Temperature Structure of Proteinase K at 38.4 keV and 0.04 MGy
- PDB DOI: https://doi.org/10.2210/pdb4B5L/pdb
- Classification: HYDROLASE
- Organism(s): Parengyodontium album
- Mutation(s): No
- Deposited: 2012-08-05 Released: 2012-08-15
Experimental Data Snapshot
- Method: X-RAY DIFFRACTION
- Resolution: 1.60 ?
- R-Value Free: 0.184
- R-Value Work: 0.158
- R-Value Observed: 0.160
Starting Model: experimental
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wwPDB Validation 3D Report Full Report
This is version 1.4 of the entry. See complete history.
Literature
To be published.
Macromolecules
Find similar proteins by:
(by identity cutoff) | 3D Structure
Entity ID: 1 | |||||
|---|---|---|---|---|---|
| Molecule | Chains | Sequence Length | Organism | Details | Image |
| PROTEINASE K | 279 | Parengyodontium album | Mutation(s): 0 EC: 3.4.21.64 |  | |
UniProt | |||||
Find proteins for P06873 (Parengyodontium album) Explore P06873 Go to UniProtKB: P06873 | |||||
Entity Groups | |||||
| Sequence Clusters | 30% Identity50% Identity70% Identity90% Identity95% Identity100% Identity | ||||
| UniProt Group | P06873 | ||||
Sequence AnnotationsExpand | |||||
| |||||
Small Molecules
| Ligands 1 Unique | |||||
|---|---|---|---|---|---|
| ID | Chains | Name / Formula / InChI Key | 2D Diagram | 3D Interactions | |
| CA Query on CA | B [auth A] | CALCIUM ION Ca BHPQYMZQTOCNFJ-UHFFFAOYSA-N |  | ||
Experimental Data & Validation
Experimental Data
- Method: X-RAY DIFFRACTION
- Resolution: 1.60 ?
- R-Value Free: 0.184
- R-Value Work: 0.158
- R-Value Observed: 0.160
- Space Group: P 43 21 2
Unit Cell:
| Length ( ? ) | Angle ( ? ) |
|---|---|
| a = 68.538 | ¦Á = 90 |
| b = 68.538 | ¦Â = 90 |
| c = 108.375 | ¦Ă = 90 |
| Software Name | Purpose |
|---|---|
| REFMAC | refinement |
| HKL-2000 | data reduction |
| HKL-2000 | data scaling |
| MOLREP | phasing |
Entry History
Deposition Data
- Released Date: 2012-08-15 Deposition Author(s): Jakoncic, J.
Revision History (Full details and data files)
- Version 1.0: 2012-08-15
Type: Initial release - Version 1.1: 2019-01-30
Changes: Data collection, Experimental preparation, Other - Version 1.2: 2019-02-06
Changes: Data collection, Experimental preparation - Version 1.3: 2023-12-20
Changes: Data collection, Database references, Derived calculations, Other, Refinement description - Version 1.4: 2024-10-16
Changes: Structure summary
